Loading .gitignore +2 −1 Original line number Diff line number Diff line Loading @@ -28,3 +28,4 @@ Selected_SEM_Images/.DS_Store Selected_SEM_Images/Electrolyzers/.DS_Store Selected_SEM_Images/Fuel_Cells/.DS_Store Selected_SEM_Images/Fuel_Cells/Non-PGM/.DS_Store .qodo Combined_4DSTEM.pdf +2.15 KiB (14.6 MiB) File changed.No diff preview for this file type. View original file View changed file Combined_4DSTEM.tex +7 −6 Original line number Diff line number Diff line Loading @@ -194,8 +194,8 @@ \end{bmatrix} = \begin{bmatrix} 1 + \epsilon_{xx} & \frac{\epsilon_{xy} - \epsilon_{\theta}}{2} \\ \frac{\epsilon_{yx} + \epsilon_{\theta}}{2} & 1 + \epsilon_{yy} 1 + \epsilon_{yy} & \frac{\epsilon_{\theta} - \epsilon_{xy}}{2} \\ -\left(\frac{\epsilon_{yx} + \epsilon_{\theta}}{2}\right) & 1 + \epsilon_{xx} \end{bmatrix} \times \begin{bmatrix} Loading Loading @@ -244,13 +244,14 @@ \subsection{\label{ssec:aberration_correction}Common Referencing to Quantify Strains Across Particles} \begin{figure*} \centering \includegraphics[width=\textwidth]{GeneratedFigures/Montage_Figure.pdf} \caption{\label{fig:montage} \textbf{Volumetric Strain across all nanoparticles. a,} \includegraphics[width=\textwidth]{GeneratedFigures/Corrected_Median_Spots.pdf} \caption{\label{fig:diff_correction} \textbf{Correcting median spots to known PtCo pattern. a,} The theoretically calculated diffraction pattern for PtCo alloy, with the peak positions and the corresponding Miller indices in red. \textbf{b,} Original median spots for \textit{beginning-of-life (BOL)} nanoparticles in red, with the corrected spots shown in blue. \textbf{c,} NOriginal median spots for \textit{end-of-life (EOL)} nanoparticles in red, with the corrected spots shown in blue.} \end{figure*} To generate the corrected strain maps, after the aberration correction, we also need to get corrected median spots. This is because our strain is calculated with respected to the median diffraction position in each nanoparticle. Thus, first we apply our aberration correction parameters to the median positions. Loading @@ -272,8 +273,8 @@ \subsection{\label{ssec:montage_strain}Volumetric Strain across all nanoparticles} \begin{figure*} \centering \includegraphics[width=\textwidth]{GeneratedFigures/Corrected_Median_Spots.pdf} \caption{\label{fig:diff_correction} \textbf{Correcting median spots to known PtCo pattern. a,} \includegraphics[width=\textwidth]{GeneratedFigures/Montage_Figure.pdf} \caption{\label{fig:montage} \textbf{Volumetric Strain across all nanoparticles. a,} The theoretically calculated diffraction pattern for PtCo alloy, with the peak positions and the corresponding Miller indices in red. \textbf{b,} Original median spots for \textit{beginning-of-life (BOL)} nanoparticles in red, with the corrected spots shown in blue. \textbf{c,} NOriginal median spots for \textit{end-of-life (EOL)} nanoparticles in red, with the corrected spots shown in blue.} Loading GeneratedFigures/04_ABF_mrads-mac136762.png 0 → 100755 +12.7 MiB Loading image diff... GeneratedFigures/04_ABF_mrads.png −12.7 MiB (0 B) File changed.No diff preview for this file type. View original file View changed file Loading
.gitignore +2 −1 Original line number Diff line number Diff line Loading @@ -28,3 +28,4 @@ Selected_SEM_Images/.DS_Store Selected_SEM_Images/Electrolyzers/.DS_Store Selected_SEM_Images/Fuel_Cells/.DS_Store Selected_SEM_Images/Fuel_Cells/Non-PGM/.DS_Store .qodo
Combined_4DSTEM.pdf +2.15 KiB (14.6 MiB) File changed.No diff preview for this file type. View original file View changed file
Combined_4DSTEM.tex +7 −6 Original line number Diff line number Diff line Loading @@ -194,8 +194,8 @@ \end{bmatrix} = \begin{bmatrix} 1 + \epsilon_{xx} & \frac{\epsilon_{xy} - \epsilon_{\theta}}{2} \\ \frac{\epsilon_{yx} + \epsilon_{\theta}}{2} & 1 + \epsilon_{yy} 1 + \epsilon_{yy} & \frac{\epsilon_{\theta} - \epsilon_{xy}}{2} \\ -\left(\frac{\epsilon_{yx} + \epsilon_{\theta}}{2}\right) & 1 + \epsilon_{xx} \end{bmatrix} \times \begin{bmatrix} Loading Loading @@ -244,13 +244,14 @@ \subsection{\label{ssec:aberration_correction}Common Referencing to Quantify Strains Across Particles} \begin{figure*} \centering \includegraphics[width=\textwidth]{GeneratedFigures/Montage_Figure.pdf} \caption{\label{fig:montage} \textbf{Volumetric Strain across all nanoparticles. a,} \includegraphics[width=\textwidth]{GeneratedFigures/Corrected_Median_Spots.pdf} \caption{\label{fig:diff_correction} \textbf{Correcting median spots to known PtCo pattern. a,} The theoretically calculated diffraction pattern for PtCo alloy, with the peak positions and the corresponding Miller indices in red. \textbf{b,} Original median spots for \textit{beginning-of-life (BOL)} nanoparticles in red, with the corrected spots shown in blue. \textbf{c,} NOriginal median spots for \textit{end-of-life (EOL)} nanoparticles in red, with the corrected spots shown in blue.} \end{figure*} To generate the corrected strain maps, after the aberration correction, we also need to get corrected median spots. This is because our strain is calculated with respected to the median diffraction position in each nanoparticle. Thus, first we apply our aberration correction parameters to the median positions. Loading @@ -272,8 +273,8 @@ \subsection{\label{ssec:montage_strain}Volumetric Strain across all nanoparticles} \begin{figure*} \centering \includegraphics[width=\textwidth]{GeneratedFigures/Corrected_Median_Spots.pdf} \caption{\label{fig:diff_correction} \textbf{Correcting median spots to known PtCo pattern. a,} \includegraphics[width=\textwidth]{GeneratedFigures/Montage_Figure.pdf} \caption{\label{fig:montage} \textbf{Volumetric Strain across all nanoparticles. a,} The theoretically calculated diffraction pattern for PtCo alloy, with the peak positions and the corresponding Miller indices in red. \textbf{b,} Original median spots for \textit{beginning-of-life (BOL)} nanoparticles in red, with the corrected spots shown in blue. \textbf{c,} NOriginal median spots for \textit{end-of-life (EOL)} nanoparticles in red, with the corrected spots shown in blue.} Loading
GeneratedFigures/04_ABF_mrads.png −12.7 MiB (0 B) File changed.No diff preview for this file type. View original file View changed file